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Fakultät BCI

Analytical Devices

Schaubild Homogeneous Catalysis

Gas Chromatography

Auto-sampling devices:

  • HP (FID/WLD)
  • Agilent (FID/WLD/MSD)
  • Shimadzu ( FID/MSD)

We use it for:

  • Quantitative and qualitative analysis of miscellaneous organic substances (polar/apolar/chiral) and gases
Bild einer Gas Chromatographie Apparatur

High Performance Liquid Chromatography

Device:

  • VWR/Hitachi

We use it for:

  • Preparation, separation, identification and quantification of non-volatile substances
  • Operation as two separate systems or continuous variation of mixing ratios of solvents
Bild einer Hochleistungsflüssigkeitschromatographie Apparatur

High Resolution Mass Spectroscopy

Device:

  • Bruker „compact QTOF“ with ESI source in the chemical department of TU Dortmund

We use it for:

  • Characterization of novel products

Inductively Coupled Plasma Optical Emission Spectrometry

Device:

  • Thermo Elemental IRIS Intrepid

We use it for:

  • Determination of catalyst leaching
Bild von einer Optische Emissionsspektrometrie mit induktiv gekoppeltem Plasma Apparatur

Infrared spectroscopy

Devices:

  • Bruker Vertex 70 (transmittance spectrum)
  • Mettler Toledo ReactIR 15 (attenuated total reflexion IR probe)

We use it for:

  • In-situ analysis
  • Real-time analysis
Bild von Infrarot Spectroscopy Apparat

Nuclear Magnetic Resonance

Devices:

  • Bruker Corp. DRX300, DRX400 and DRX500 or ARX300 devices in the chemical department of TU Dortmund
  • SPINSOLVE PHOSPHORUS 60 MHz ULTRA (1H,19F and 31P) portable benchtop NMR device

We use it for:

  • Real-time reaction monitoring
  • Short-term analysis of purified products
  • Solvent supression
Bild einer Magnetische Kernresonanz Apparatur

Ultraviolet-Visible Spectroscopy

Devices:

  • Varian Cary 100

We use it for:

  • Evaluation of separation techniques
  • Quantification of catalyst leaching
Bild von Ultraviolett-Visuelle Spektroskopie Apparatur

Melting Point Apparatus

Bild von Melting Point Apparat

Coulometry

Devices:

  • TitroLine 7500 KF trace

We use it for:

  • According to Karl Fischer for water determination in organic solvents
Bild von Coulometry Apparat

Refractometer

Devices:

  • Zeiss

We use it for:

  • Determination of the refractive index
Bild von Refractometer

Microwave

Devices:

  • Mars 6

We use it for:

  • Chemical digestions for ICP analysis
Bild von Aufschlussmikrowelle