Reaction Equipment
Autoclaves
Autoclaves:
- Different sizes of stainless steel autoclaves à 25 mL to 5000 mL, leakproof up to 150 bar
- Different Sizes of Glass autoclaves à 20 mL to 200 mL, leakproof up to 10 bar
- Special reactor concepts: Glass window reactor, Jet-Loop Reactor, Taylor Couette Reactor, ATR-probe reactor, IR-glass window reactor
We use it for:
- Pressure Experiments
- Getting insight in the phase behaviour of biphasic mixtures
- Investigating influence of reactor concept on the reaction performance in biphasic mixtures
- Investigating the reaction in situ by ATR measurements
Dosing and Sampling
Dosing:
- Gases (hydrogen, carbon monoxide, syngas, argon, nitrogen)
- Liquid gases (ammonia, butadiene, isobutene)
- Liquids (continuos dosing over HPLC-pump)
Sampling:
- Gases → gas uptake measurements over mass flow indicators
- Liquids → automatic sampling system
- Online GC → automated measurements of the reaction system
We use it for:
- Investigations in the reaction performance of liquid gases
- Kinetic measurements
- Monitoring of continous experiments in miniplant scale
Purification and Recovery
Purification methods:
- Distillable compounds à Kugelrohr- / Spaltrohrdistillation, large distillation column
- Column chromatography
- Preparative HPLC column
Recovery methods:
- Monophasic systems à crystallization, membranes
- Biphasic systems à decanter, extractors (e.g. rotating disc contactor)
- Online GC à automated measurements of the reaction system
We use it for:
- Purification of value products
- Recovery of precious transition metal catalysts